Proceedings of the 2nd International Conference on Contemporary Science and Clinical Pharmacy 2021 (ICCSCP 2021)

Various Chloride Salt Addition in Mesoporous Material (SBA-15) Synthesis and Potential as Carrier for Dissolution Enhancer

Authors
Uswatul Hasanah1, 2, *, Saleh Wikarsa2, Sukmadjaja Asyarie2
1Faculty of Pharmacy, Universitas Andalas, Padang 25163, West Sumatra, Indonesia
2School of Pharmacy, Bandung Institute of Technology, Bandung 40132, West Java, Indonesia
*Corresponding author. Email: uswatulhasanah@phar.unand.ac.id
Corresponding Author
Uswatul Hasanah
Available Online 17 November 2021.
DOI
10.2991/ahsr.k.211105.050How to use a DOI?
Keywords
Mesoporous material; SBA-15; atorvastatin Ca; dissolution
Abstract

Nano pores in Santa Barbara Amorphous (SBA-15) has potential to be employed as a carrier to enhance solubility and dissolution. Addition of salt on surfactant solution enabling the SBA-15 synthesis process carried on room temperature instead of 35-50°C. Atorvastatin Ca, which belongs to Biopharmaceuticals Classification System (BCS) class II, has low solubility in water, was used as a model drug. SBA-15 was synthetized using Pluronic P123:H2O:HCl:TEOS on 0.02:166:6:1 molar proportion with addition of 6 moles of inorganic salts: NaCl, KCl, MgCl2, and CaCl2. SBA-15 was impregnated to drug solution in methanol with SBA-15:ATV proportion of 1:1 before it was evaporated. The unloaded and loaded mesoporous were characterized with DTA, pXRD, FT-IR, BET and SEM. The result showed the highest surface area achieved by MgCl2 addition as 724.227 m2/g, meanwhile the biggest pore size and pore volume achieved was by the addition of KCl as 5.411 nm and 8,948 x 10-1 cm3/g. The dissolved amount in phosphate buffer 0.05 M pH 6.8 showed the significance enhancement by 2.5 to 6-fold at 5 min in comparison with intact atorvastatin Ca. In conclusion, the properties of SBA-15 vary with the addition of different salts, and can be used to enhance the dissolution of atorvastatin Ca.

Copyright
© 2021 The Authors. Published by Atlantis Press International B.V.
Open Access
This is an open access article under the CC BY-NC license.

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Volume Title
Proceedings of the 2nd International Conference on Contemporary Science and Clinical Pharmacy 2021 (ICCSCP 2021)
Series
Advances in Health Sciences Research
Publication Date
17 November 2021
ISBN
978-94-6239-450-6
ISSN
2468-5739
DOI
10.2991/ahsr.k.211105.050How to use a DOI?
Copyright
© 2021 The Authors. Published by Atlantis Press International B.V.
Open Access
This is an open access article under the CC BY-NC license.

Cite this article

TY  - CONF
AU  - Uswatul Hasanah
AU  - Saleh Wikarsa
AU  - Sukmadjaja Asyarie
PY  - 2021
DA  - 2021/11/17
TI  - Various Chloride Salt Addition in Mesoporous Material (SBA-15) Synthesis and Potential as Carrier for Dissolution Enhancer
BT  - Proceedings of the 2nd International Conference on Contemporary Science and Clinical Pharmacy 2021 (ICCSCP 2021)
PB  - Atlantis Press
SP  - 343
EP  - 349
SN  - 2468-5739
UR  - https://doi.org/10.2991/ahsr.k.211105.050
DO  - 10.2991/ahsr.k.211105.050
ID  - Hasanah2021
ER  -