Proceedings of the 1st Nusa Tenggara International Conference on Chemistry (NITRIC 2022)

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Lichen Dirinaria Applanata Microwave Assisted Extraction Using Deep Eutectic Solvents and Binary Solvents

Authors
Misbahu Said Ahmad1, *, Zaharraddeen Muhammed1
1Sule Lamido University, Kano, Nigeria
*Corresponding author. Email: misbahus.ahmad@slu.edu.ng
Corresponding Author
Misbahu Said Ahmad
Available Online 14 April 2023.
DOI
10.2991/978-94-6463-130-2_3How to use a DOI?
Keywords
Deep Eutectic Solvent; Ionic liquid; Lichen; Green chemistry; binary solvent
Abstract

Ionic liquids and volatile organic solvents are both intended to be replaced with deep eutectic solvents (DES) in industrial and laboratory procedures. Low cost, simple manufacturing, biodegradability, strong solubilization strength, and low toxicity are a few advantages of using DES. One of the most crucial areas in green chemistry is the emergence of DES. Lichens, on the other hand, produce Secondary Metabolites with distinctive properties (SM). These SM exhibit a range of biological actions, such as anti-tumor, anti-inflammatory, and antioxidant qualities. This study focuses on the Microwave Assisted Extraction (MAE) of the SM from the lichen Dirinaria applanata utilizing a Binary Solvent (BS) of acetone and ChCl:Urea and DES constructed of chloroform and urea. 1,4-butanediol. The advantage of MAE is faster extraction times and less solvent usage. At 100 W, the MAE was run for 60, 120, 180, 240, and 300 s. The separation of the numerous Secondary Metabolites (SM) from the lichen Dirinaria applanata was observed using thin layer chromatography (TLC). The greatest yield (%) of MAE employing ChCl:Urea after 240 s was 22.95%. The ChCl:1,4-butanediol extraction yield (%) when employing a binary solvent (BS) is comparable to that of acetone-based normal soaking extraction (NSE). Using BS and DES as solvents in MAE offers a more affordable option than the standard soaking extraction method that uses acetone. To identify and describe the secondary metabolites obtained from the lichen Dirinaria applanata, more investigation must be conducted.

Copyright
© 2023 The Author(s)
Open Access
Open Access This chapter is licensed under the terms of the Creative Commons Attribution-NonCommercial 4.0 International License (http://creativecommons.org/licenses/by-nc/4.0/), which permits any noncommercial use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license and indicate if changes were made.

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Volume Title
Proceedings of the 1st Nusa Tenggara International Conference on Chemistry (NITRIC 2022)
Series
Atlantis Highlights in Chemistry and Pharmaceutical Sciences
Publication Date
14 April 2023
ISBN
978-94-6463-130-2
ISSN
2590-3195
DOI
10.2991/978-94-6463-130-2_3How to use a DOI?
Copyright
© 2023 The Author(s)
Open Access
Open Access This chapter is licensed under the terms of the Creative Commons Attribution-NonCommercial 4.0 International License (http://creativecommons.org/licenses/by-nc/4.0/), which permits any noncommercial use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license and indicate if changes were made.

Cite this article

risenwbib
TY  - CONF
AU  - Misbahu Said Ahmad
AU  - Zaharraddeen Muhammed
PY  - 2023
DA  - 2023/04/14
TI  - Lichen Dirinaria Applanata Microwave Assisted Extraction Using Deep Eutectic Solvents and Binary Solvents
BT  - Proceedings of the 1st Nusa Tenggara International Conference on Chemistry (NITRIC 2022)
PB  - Atlantis Press
SP  - 13
EP  - 19
SN  - 2590-3195
UR  - https://doi.org/10.2991/978-94-6463-130-2_3
DO  - 10.2991/978-94-6463-130-2_3
ID  - Ahmad2023
ER  -