The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid
Authors
Liping Wang, Diandian Deng, Hewei Yan, Xiaoxia Sun, Chaochao Wei
Corresponding Author
Liping Wang
Available Online May 2016.
- DOI
- 10.2991/ifeesd-16.2016.142How to use a DOI?
- Keywords
- 2,3-dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid, organic light-emmitting material, synthesis, -conjugated polymers
- Abstract
A new synthetic approach to synthesize 2,3-dimethyl -2,3-dihydrofuro [3,4-b][1,4] dioxine-5,7 -dicarboxylic acid from a common precursor diglycolic acid was reported. Starting from the commercial material diethylene glycol, diethyl oxalate and 2,3-dibromobutane, the compound was synthesized through oxidation reaction, acylation, hydrolysis and elimination reaction with moderate yield via a five-step reaction. The procedure was described herein with several advantages, including high product yields and easy purification.
- Copyright
- © 2016, the Authors. Published by Atlantis Press.
- Open Access
- This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).
Cite this article
TY - CONF AU - Liping Wang AU - Diandian Deng AU - Hewei Yan AU - Xiaoxia Sun AU - Chaochao Wei PY - 2016/05 DA - 2016/05 TI - The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid BT - Proceedings of the 2016 International Forum on Energy, Environment and Sustainable Development PB - Atlantis Press SP - 776 EP - 779 SN - 2352-5401 UR - https://doi.org/10.2991/ifeesd-16.2016.142 DO - 10.2991/ifeesd-16.2016.142 ID - Wang2016/05 ER -