Determination flavomycin residue in grass carp by high performance liquid chromatography

DOI

10.2991/ic3me-15.2015.91How to use a DOI?

Keywords

High performance liquid chromatography; grass carp;flavomycin; residues;

Abstract

A method for the determination of flavomycin in shrimp by high performance liquid chromatography was established. Flavomycin in sample was extracted by methanol solution and defatted with n-hexane. The lower was cleaned through the membrane and determined by HPLC. The calibration curve was linear. The method was accurate and reproducible, being successfully applied to the monitoring of flavomycin in grass carp. The recoveries were 83.9 %-88.2 % in the spiked range of 2.0-50.0 mg/kg in grass carp. The relative standard deviation was below 10.4%. The limit of detection for this method as defined by ten times signal to noise was 2.0mg/kg.

Copyright

© 2015, the Authors. Published by Atlantis Press.

Open Access

This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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TY  - CONF
AU  - Liang-Liang Tian
AU  - Dong-Mei Huang
AU  - Yong-Fu Shi
AU  - Feng Han
AU  - Peng Zhou
PY  - 2015/08
DA  - 2015/08
TI  - Determination flavomycin residue in grass carp by high performance liquid chromatography
BT  - Proceedings of the 3rd International Conference on Material, Mechanical and Manufacturing Engineering
PB  - Atlantis Press
SP  - 462
EP  - 465
SN  - 2352-5401
UR  - https://doi.org/10.2991/ic3me-15.2015.91
DO  - 10.2991/ic3me-15.2015.91
ID  - Tian2015/08
ER  -