Proceedings of the 4th Forum in Research, Science, and Technology (FIRST-T1-T2-2020)

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Effect of Sulfonation Temperature and Time on the Preparation of Methyl Ester Sulfonate Surfactant From Crude Palm Oil (CPO) Based Methyl Ester

Authors
Jaksen, Idha Silviyati, Endang Supraptiah, Rima Daniar, Elina Margaretty
Corresponding Author
Jaksen
Available Online 9 February 2021.
DOI
10.2991/ahe.k.210205.018How to use a DOI?
Keywords
CPO, Methyl Ester, Methyl Ester Sulfonate, Sulfonation, Surfactants
Abstract

Research to study the effect of temperature and sulfonation time on the preparation of Methyl Ester Sulfonate (MES) surfactant using CPO-based Methyl Ester (ME) as raw material has been carried out. The temperature was varied 80 oC, 90 oC and 100 oC; while the observation time is carried out every 1 hour to 4 hours. The sulfonating agent was used Na2S2O5 where the mole ratio of ME and the agent was fixed, as well as the type and concentration of the catalyst. The experimental method was carried out in stages starting from sulfonation, bleaching, neutralization, filtering, drying MES, analysis and testing. The best experimental results were obtained at a temperature of 100 oC and a sulfonation time of 4 hours with the resulting MES characteristics, namely iodine number 16.92 g iod / g sample, acid number 4.45 mg KOH / g sample, surface tension 27.4 dyne / cm, and emulsion stability of 50.8 minutes. The best characteristics of Methyl Ester Sulfonate Acid (MES) are density 0.83-0.92 gr / ml, viscosity 1.35 - 2.35 cp, and pH 2.26-4.68.

Copyright
© 2021, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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Volume Title
Proceedings of the 4th Forum in Research, Science, and Technology (FIRST-T1-T2-2020)
Series
Atlantis Highlights in Engineering
Publication Date
9 February 2021
ISBN
978-94-6239-332-5
ISSN
2589-4943
DOI
10.2991/ahe.k.210205.018How to use a DOI?
Copyright
© 2021, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

Cite this article

risenwbib
TY  - CONF
AU  - Jaksen
AU  - Idha Silviyati
AU  - Endang Supraptiah
AU  - Rima Daniar
AU  - Elina Margaretty
PY  - 2021
DA  - 2021/02/09
TI  - Effect of Sulfonation Temperature and Time on the Preparation of Methyl Ester Sulfonate Surfactant From Crude Palm Oil (CPO) Based Methyl Ester
BT  - Proceedings of the 4th Forum in Research, Science, and Technology (FIRST-T1-T2-2020)
PB  - Atlantis Press
SP  - 95
EP  - 102
SN  - 2589-4943
UR  - https://doi.org/10.2991/ahe.k.210205.018
DO  - 10.2991/ahe.k.210205.018
ID  - 2021
ER  -