Synthesis and Characterization of (-)-Dibornyl Oxalate

DOI

10.2991/ic3me-15.2015.86How to use a DOI?

Keywords

(-)-Borneol, Oxalyl Chloride, (-)-Dibornyl oxalate, Characterization

Abstract

(-)-Dibornyl oxalate was synthesized by the reaction of natural (-)-borneol with oxalyl chloride under the optimized reaction conditions: temperature 35 , time 1 h and the molar ratio of (-)-borneol and oxalyl chloride 1.0 : 0.6. The reaction underwent in good selectivity as 99 % for target product which can be easily purified to 99.9 % through recrystallization. The structure of (-)-dibornyl oxalate was characterized by GC-MS, FT-IR, 1H NMR and 13C NMR.

Copyright

© 2015, the Authors. Published by Atlantis Press.

Open Access

This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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TY  - CONF
AU  - Xiaomin Yuan
AU  - Zhendong Zhao
AU  - Shichao Xu
AU  - Yuxiang Chen
AU  - Liangwu Bi
PY  - 2015/08
DA  - 2015/08
TI  - Synthesis and Characterization of (-)-Dibornyl Oxalate
BT  - Proceedings of the 3rd International Conference on Material, Mechanical and Manufacturing Engineering
PB  - Atlantis Press
SP  - 437
EP  - 440
SN  - 2352-5401
UR  - https://doi.org/10.2991/ic3me-15.2015.86
DO  - 10.2991/ic3me-15.2015.86
ID  - Yuan2015/08
ER  -